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Deisobutanizer / Butane Splitter Calculator

GPSA Ch. 16 / GPA 2140

Deisobutanizer / Butane Splitter Calculator
Sizes deisobutanizer (butane splitter) fractionation columns for the close-boiling iC₄/nC₄ separation. This is one of the most difficult separations in NGL processing due to the very low relative volatility (α ≈ 1.1–1.3), requiring high tray counts and high reflux ratios. Calculates minimum stages, minimum reflux ratio, actual trays, column diameter, and reboiler/condenser duties per GPSA Ch. 16 and GPA 2140.
GPSA Ch. 16 GPA 2140
Calculation Mode:
Design: Size butane splitter from feed composition and product specifications.

Feed Conditions

BPD
°F
psig

Feed Composition (mol%)

Light end from debutanizer

Product Specifications

mol%
mol%

Column Design Parameters

%
in
%

Typical Butane Splitter Operating Conditions

Parameter Range
Pressure60–100 psig
Overhead Temp90–130°F
Bottoms Temp140–180°F
Reflux Ratio5–15
Trays60–120

Engineering Basis

Fenske Equation (Minimum Stages):

Nmin = ln[(xLK,D / xHK,D)(xHK,B / xLK,B)] / ln(α)

Where xLK,D = light key (iC₄) mole fraction in distillate, xHK,B = heavy key (nC₄) mole fraction in bottoms, α = average relative volatility of iC₄ to nC₄ (typically 1.1–1.3).

Gilliland Correlation:

(N − Nmin) / (N + 1) = f[(R − Rmin) / (R + 1)]

Correlates actual stages N to actual reflux ratio R given minimum stages Nmin and minimum reflux Rmin from the Underwood equation.

Underwood Equation: Determines minimum reflux ratio Rmin from feed composition, feed condition (q), and relative volatilities. Combined with Gilliland correlation to find actual stages at the design reflux multiplier.

Column Diameter: Sized from vapor/liquid traffic using Fair’s flooding correlation at the design flood fraction.

Design Guidelines

Close-Boiling Separation: The iC₄/nC₄ separation has α ≈ 1.1–1.3, requiring 60–120 trays and reflux ratios of 5–15. This is one of the most energy-intensive columns in NGL processing.
Structured Packing: Due to the high tray count, structured packing is often considered to reduce column height by 30–50% compared to trayed columns.
iC₄ Applications: Isobutane overhead product is primarily used as alkylation unit feed, refrigerant (R-600a), and aerosol propellant.

Frequently Asked Questions

Why is iCβ‚„/nCβ‚„ separation difficult?

The isobutane/normal butane separation is one of the most difficult in NGL processing because the relative volatility is very low (Ξ± β‰ˆ 1.1–1.3). This requires high tray counts and high reflux ratios, making the butane splitter an energy-intensive column.

What shortcut method does the butane splitter calculator use?

The calculator uses the Fenske-Underwood-Gilliland shortcut method to determine minimum stages (Fenske equation), minimum reflux ratio (Underwood), and actual trays at operating reflux (Gilliland correlation) per GPSA Ch. 16.

What is the Fenske equation used for?

The Fenske equation calculates the minimum number of theoretical stages required for a given separation at total reflux. It uses the light key and heavy key mole fractions in distillate and bottoms with the average relative volatility.

What product specifications does a butane splitter achieve?

A typical butane splitter produces an isobutane overhead product with 95–99% purity and a normal butane bottoms product. The calculator allows user-defined purity targets and computes the required stages, reflux, and column dimensions per GPSA Ch. 16 and GPA 2140.